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  grilamid processing issues

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Author Topic:   grilamid processing issues
paddy66
Member

Posts: 3
From:ireland
Registered: Feb 2007

posted February 02, 2007 07:40 PM     Click Here to See the Profile for paddy66     Edit/Delete Message   Reply w/Quote
we are curently having a lot of difficulties processing grilamid L25 in a 3/4 inch extruder, unstable melt pressure,m/c amps erratic and inconsistant feed leading to tubing with unstable od, have tried various different screws,melt and throat temps, speeds etc without much success, any advice would be appreciated.

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Steve H
Moderator

Posts: 401
From:Christchurch,New Zealand
Registered: Jun 2001

posted February 03, 2007 12:24 AM     Click Here to See the Profile for Steve H     Edit/Delete Message   Reply w/Quote
Welcome to the single screw forum.

What LD is your extruder, screw geometery? are you running screen packs, what melt pressure are you getting.

------------------
Steve Hodgson

If at first you don't succeed, skydiving is not for you.

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paddy66
Member

Posts: 3
From:ireland
Registered: Feb 2007

posted February 06, 2007 06:06 PM     Click Here to See the Profile for paddy66     Edit/Delete Message   Reply w/Quote
hey steve, extruder ld 24, various screws used e.g standard 3:1 metering, pebax mixer, low volume with deeper feed section than standard metering screw, generally up to 200 mesh used, melt pressure varies depending on tooling in head but generally 1500 to 3000 is ideal on this extruder,have ran other nylons sucessfully to a tight tolerance on this extruder cannot understand what the problem with grilamid is, thanks for your interest.

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Tom C
Moderator

Posts: 834
From:Brodheadsville, PA USA
Registered: Jun 2001

posted February 08, 2007 09:26 AM     Click Here to See the Profile for Tom C     Edit/Delete Message   Reply w/Quote
Sounds like a feeding issue.

Try this;

Set the first zone to as cold as possible and the throat water full on and let it stabilize for at least 4 hours.

Turning the screw slowly, add the resin. See if you get a steady strong output. If not, slowly raise the first zone until you acheive steady output. Record the zone temperature that you get the highest amps draw.

Start with the above procedure again with the extruder stopped and the first zone cold again for 4 hours. Start the extruder at the desired RPMs. Set the first zone to the above established temperature and wait for the first zone to heat up. The process should run well when the first zone temperature is acheived.

You may find that after some period of time the process begins to become erratic. If this occurs, then you need screw cooling up to the end of the first zone.

If none of this works, send me an email.


------------------
Best Regards,

Tom Cunningham

www.ExtrusionTechnicalServices.com

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paddy66
Member

Posts: 3
From:ireland
Registered: Feb 2007

posted March 15, 2007 05:49 PM     Click Here to See the Profile for paddy66     Edit/Delete Message   Reply w/Quote
Thanks for your suggestion, feed has improved slightly but still very erratic which is very puzzling as nylon 11 (vestamid) and grilamid compounded with a small percentage eva lubricant both run very well easily holding tolerance of +/- 0.02mm. I was wondering if there is any particular design of throat section or screw that is helpfull when processing this material, any thoughts you have would be appreciated.

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Tom C
Moderator

Posts: 834
From:Brodheadsville, PA USA
Registered: Jun 2001

posted March 15, 2007 07:37 PM     Click Here to See the Profile for Tom C     Edit/Delete Message   Reply w/Quote
I really don't know anything specific about this material. I'm just giving you basic extrusion troubleshooting tips.

Melting point is 352F

How do your amps look?
What type of screw do you have?
How many RPMs
Temperature settings?
Is your extruder worn?


Processing Properties from Matweb;

Processing Temperature 240 - 250 °C 464 - 482 °F Compression Zone
Processing Temperature 60 - 90 °C 140 - 194 °F Hopper Zone
Processing Temperature 240 - 250 °C 464 - 482 °F Metering Zone
Feed Temperature 230 - 240 °C 446 - 464 °F
Nozzle Temperature 230 - 240 °C 446 - 464 °F
Melt Temperature 230 - 250 °C 446 - 482 °F
Head Temperature 240 - 250 °C 464 - 482 °F
Drying Temperature Max 80 °C Max 176 °F Desiccant Drye

Oh yes, and what is the size of the pellets relative to the depth of the screw in the feed section?

------------------
Best Regards,

Tom Cunningham
www.ExtrusionTechnicalServices.com

[This message has been edited by Tom C (edited March 15, 2007).]

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Stephen J. Derezinski
Senior Member

Posts: 64
From:Penfield, NY, 14526, USA
Registered: Apr 2003

posted March 23, 2007 08:38 AM     Click Here to See the Profile for Stephen J. Derezinski     Edit/Delete Message   Reply w/Quote
Feed hopper bridging, perhaps?
Try a wide range of feed hopper levels.

------------------
Steve Derezinski, Ph.D.
Extruder Tech, Inc.
steve@extrudertech.com
www.extrudertech.com

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alpertl
Senior Member

Posts: 55
From:Dayville, CT USA
Registered: May 2002

posted March 27, 2007 03:01 PM     Click Here to See the Profile for alpertl     Edit/Delete Message   Reply w/Quote
quote:
Originally posted by paddy66:
we are curently having a lot of difficulties processing grilamid L25 in a 3/4 inch extruder, unstable melt pressure,m/c amps erratic and inconsistant feed leading to tubing with unstable od, have tried various different screws,melt and throat temps, speeds etc without much success, any advice would be appreciated.

Try a low compression type screw, maybe 1.5:1 with a deep feed section, if you have one.

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