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Author Topic:   monofilament research project
kyry
Member

Posts: 3
From:Urbana, IL, USA
Registered: Mar 2004

posted March 02, 2004 11:14 PM     Click Here to See the Profile for kyry     Edit/Delete Message   Reply w/Quote
Hi,

I have this research project to do, where an important part is to extrude a 30 microns monofilament of ceramic powder. Using a Chemat Fiber extruder with a 30 microns die, and I always get phase separation and/or too thick fibers (thicker than the die).

any ideas on improving the formulation?

powder (micron size particles ) 38 wt%
Water 60 wt%
Methocel (Dow Chemical cellulose) 2 wt %

thanks


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zabielski
Senior Member

Posts: 284
From:McHenry, IL USA
Registered: Nov 2002

posted March 03, 2004 05:19 AM     Click Here to See the Profile for zabielski   Click Here to Email zabielski     Edit/Delete Message   Reply w/Quote
So what is the average micron size of the powder your using? 38% by weight does not tell us anything.

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kyry
Member

Posts: 3
From:Urbana, IL, USA
Registered: Mar 2004

posted March 03, 2004 11:59 AM     Click Here to See the Profile for kyry     Edit/Delete Message   Reply w/Quote
hi, sorry for the confussion in the data. the average particle size is 1.59 microns

thanks

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zabielski
Senior Member

Posts: 284
From:McHenry, IL USA
Registered: Nov 2002

posted March 04, 2004 06:18 AM     Click Here to See the Profile for zabielski   Click Here to Email zabielski     Edit/Delete Message   Reply w/Quote
OK! So now, if the "average" partical size is 1.59 micron, find out what the "top cut" is. It sounds to me that the partical size "top cut" (largest particals relative to the average)is the cause of your problem.

I think you need to do an analysis of the partical sizes available. You want a very controlled particle size. With the Lot # provided by your supplier - contact them for this information.

Relate the problems your encountering, as I seriously think that the powder is perhaps trash.

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kyry
Member

Posts: 3
From:Urbana, IL, USA
Registered: Mar 2004

posted March 04, 2004 04:59 PM     Click Here to See the Profile for kyry     Edit/Delete Message   Reply w/Quote
thanks!

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