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  Unsolved gel problem !

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Author Topic:   Unsolved gel problem !
poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 16, 2005 02:27 PM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
I work with a twin (1½") screw extruder. The extruder includes a melt pump, a vacuum pump, a polymer feeder, an additive feeder connected to a side stuffer, and a 20-40-10µm-40 screen pack on the braker plate. Lately I've been getting a lot of gels, specially after one or two day shutdowns. The funny thing is that we have been operating the same way for about two years without any special precaution. We always stopped after emptying the extruder and we closed the heating. When we started again we only had to purge 10 or 15 minutes and the flow was perfectly clear.

I'm not sure if the gels are crosslinked or unmelted polymer. We have tested the polymer but haven't found anything special. I'm not sure though that we have the right expertise to analyze the polymer correctly. What puzzles me is that we haven't changed anything. Could it be the polymer itself, or something to do with the process? Of course it would seem logical to get crosslinked gels from stagnated polymer overheating while reheating the extruder. But, we have never had any problems before. Is there something the polymer supplier can hide from us? Perhaps to much reclaim in their polymer? How would it react in our extruder? If we analyze it, will it show gels or will we see it only in the extruder? How can we know that the polymer contains reclaim? Darker color?

Thank you

[This message has been edited by poly (edited January 16, 2005).]

[This message has been edited by poly (edited January 16, 2005).]

[This message has been edited by poly (edited January 16, 2005).]

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Tom C
Moderator

Posts: 443
From:Brodheadsville, PA USA
Registered: Jun 2001

posted January 16, 2005 08:49 PM     Click Here to See the Profile for Tom C   Click Here to Email Tom C     Edit/Delete Message   Reply w/Quote
Poly,

Two thoughts;

1) Examine the materials microscopically as raw material, extruded without screens, contaminates on the screen and product. This will tell you the source.

2) Sounds as if you might have wear in your extruder. This will allow a film of material to reside on the barrel and/or screws and nor purge out. This film can degrade during the startup and shutdown. I can help with wear measurement devices if you are interested.

Tom C
www.ExtrusionTechnicalServices.com

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poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 16, 2005 09:06 PM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
Thanks for your reply.

Anything you can provide will be of great help to me.

Best regards

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poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 17, 2005 03:42 PM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
I just noticed today that the gases going through the vacuum line seems to condensate. Maybe when I stopped the vacuum pump during a shut down, this condensate might have dripped by gravity into the extruder, thus producing gels. It's a guess. I will further investigate this.

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poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 18, 2005 08:42 AM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
We finally ruled out the raw material as a possible culprit for our gel problem. We are still conducting tests.

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poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 18, 2005 08:47 AM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
Another thing... After investigation, the polymer doesn't contain reclaim. The gels are of the crosslinked type.

Are we having wear in the extruder? It's a possibility because one of our additives is very corrosive.

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Tom C
Moderator

Posts: 443
From:Brodheadsville, PA USA
Registered: Jun 2001

posted January 18, 2005 01:40 PM     Click Here to See the Profile for Tom C   Click Here to Email Tom C     Edit/Delete Message   Reply w/Quote
Best way to find out about the wear and/or corrosion problem is to pull the machine apart, inspect and measure it. Please email me if you are interested in measurment devices or an inspection service.

Tom Cunningham
www.ExtrusionTech.com

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poly
Senior Member

Posts: 6
From:Canada
Registered: Jan 2005

posted January 19, 2005 12:02 PM     Click Here to See the Profile for poly   Click Here to Email poly     Edit/Delete Message   Reply w/Quote
Mr. Cunningham,

Unfortunately, I don't have the authority to hire you. I'm only an extrusion operator.

I'm living the eternel battle between operators and engineers. I work with young green engineers freshly out of school. They have a lot to prove...

I've been an operator for 20 years and I know how an extruder works. I have also dealth with gels before. This company is so narrow minded when it comes to listenning to other people's opinions.

I don't think I will be able to convince them to hire you or anybody else for that matter.

Yesterday, as usual, they decided to patch the problem instead of finding the cause. We purged the extruder at lower temperatures before shutdown (everybody already knows this procedure!). After 7 hours of shutdown, we restarted again and the flow seemed pretty clear. As I'm killing myself to make them understand, we'll never know the cause if we keep working like this. I reminded them many times that for the past 2 years we never had this problem. Why now?

I think next time I get another problem with the process, I will leave it to them and sit down comfortably in the cafeteria while they find the solution (even if I now for sure what is the solution)!

Thank you for your offer.

Best regards

[This message has been edited by poly (edited January 19, 2005).]

[This message has been edited by poly (edited January 19, 2005).]

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Tom C
Moderator

Posts: 443
From:Brodheadsville, PA USA
Registered: Jun 2001

posted January 19, 2005 02:33 PM     Click Here to See the Profile for Tom C   Click Here to Email Tom C     Edit/Delete Message   Reply w/Quote
Poly,

It would be nice if your organization appreciated your concern. I have worked at all levels within companies, and I know exactly what you are talking about. In fact the operators complain about the engineers, the engineers about the operators and the mechanics complain about everyone!

Fact is extruders are very hard to run, control, and diagnose when there are problems. It has taken me 20+ years to start to get a handle on things, and that is with the assistance of hundres of thousands of dollars worth of training and software.

There are plenty of problems and failures to go around if you spend enough time with extruders. Hats off to anyone who has the guts to stick it out.

I'm here to help if I can.

Tom Cunningham
www.ExtrusionTechnicalServices.com

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